Chapter 2 Methodology Prepare 6 slides

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This methods-focused presentation outlines the synthesis and validation strategy for single-phase orthorhombic YFeO3. It compares multiple preparation routes, then experimentally contrasts HTSSR and LTSSR by controlling dwell time while varying precursor chemistry and calcination temperature. XRD, Rietveld refinement, and phase-fraction analysis guide route selection, identifying LTSSR as optimal. Subsequent structural, chemical, thermal, dielectric, impedance, modulus, and AC conductivity...