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Explore the potential of DMMT-based polyesters as an alternative to PET. The study delves into the synthesis from biomass, showcasing a scalable and sustainable D-A reaction method with focus on Henkel rearrangement. Achieving high molecular weight polyesters like PEmT, PPmT, and PBmT, these materials demonstrate comparable thermal stability to PET with remarkable gas barrier properties suitable for packaging. Analytical data provides insights into their mechanical strengths, crystallinity,...